Upgrade of JCNS SANS instrument KWS-2 for improved performance and beam-time efficiency

¹ Jülich Centre for Neutron Science (JCNS) at Heinz Maier-Leibnitz Zentrum (MLZ), Forscungszentrum Jülich, 85748 Garching, Germany
² Theoretical and Physical Chemistry Institute, National Hellenic Research Foundation, 11635 Athens, Greece

^* Corresponding author: a.radulescu@fz-juelich.de

Published online: 9 October 2023

Abstract

KWS-2 is a classical small angle neutron diffractometer where, following recent upgrades, the pinhole mode with different neutron-wavelengths and detector distances can be combined with focusing mode with MgF₂ lenses to reach a wide Q-range between 2x10⁻⁴ and 1.0 Å⁻¹. Further upgrades of the detection system and sample positioning system are currently in progress. A wide-angle detection prototype is currently being tested and optimized aiming at measurement conditions over an extended Q-range up to 2.0 Å⁻¹, which will be beneficial for semi-crystalline materials and small biological morphologies. The high neutron flux provided by the FRMII reactor and transported by the optimized neutron guidance system requires an adjustment of the measurement routine for a more rational use of the beam time. A new versatile in-beam sample positioning system, which includes a multi-position carousel with temperature control, robotic elements, and a storage pool for sample cuvettes, has just been installed at the instrument’s sample position. This allows the instrument to be continuously supplied with samples and provides the ability to combine experiments on similar samples or topics into a common long experimental session. Here we report in detail on the expanded Q-range option of the KWS-2 from the perspective of current performance and planned upgrades, as well as the new sample positioning system with robotic elements.